반응 #168442

반응 방정식

methyl 3-ethylcyclopent-1-enecarboxylate

→

methyl 3-ethylcyclopentanecarboxylate

용매

methanol

반응 조건

후처리

1. 1
   기타the mixture was purged with hydrogen for 10 minutes
2. 2
   기타Then reaction mixture
3. 3
   여과The reaction mixture was then filtered through a pad of celite
4. 4
   농축the filtrate was concentrated to dryness

실험 절차

To a stirred solution of methyl 3-ethylcyclopent-1-enecarboxylate (1.60 g, 10.3 mmol) in methanol (15 mL) was added 10% Pd/C (100 mg), and the mixture was purged with hydrogen for 10 minutes. Then reaction mixture was then stirred at room temperature for 16 hours under a hydrogen atmosphere (balloon). The reaction mixture was then filtered through a pad of celite, and the filtrate was concentrated to dryness to afford methyl 3-ethylcyclopentanecarboxylate as a mixture of cis and trans isomers.

출처