반응 #1677

반응 방정식

p-chlorobenzoic hydrazide

chloroacetyl chloride

→

N'-chloroacetyl-4-chlorobenzoic hydrazide

용매

dioxane

반응 조건

후처리

1. 1
   온도The resulting mixture was refluxed for three hours
2. 2
   여과filtered
3. 3
   세척The resulting solid was washed with ethyl ether
4. 4
   기타dried

실험 절차

To a solution of p-chlorobenzoic hydrazide (11.2 g) in dioxane (100 ml) was added chloroacetyl chloride (6 ml). The resulting mixture was refluxed for three hours, cooled to room temperature and filtered. The resulting solid was washed with ethyl ether and dried to yield N'-chloroacetyl-4-chlorobenzoic hydrazide as white solid.

출처