반응 #1671965

ord-9efc292a494e48d6bcb1e98cbcd01541

반응 방정식

CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1cc(C2OCCCO2)c2occc2c1
tributyl-(7-[1,3]dioxan-2-yl-benzofuran-5-yl)-stannane
Cc1noc(C)c1Br
4-bromo-3,5-dimethylisoxazole
→
Cc1noc(C)c1-c1cc(C=O)c2occc2c1
5-(3,5-Dimethyl-isoxazol-4-yl)-benzofuran-7-carbaldehyde

반응물

CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1cc(C2OCCCO2)c2occc2c1
tributyl-(7-[1,3]dioxan-2-yl-benzofuran-5-yl)-stannane
Cc1noc(C)c1Br
4-bromo-3,5-dimethylisoxazole

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

From tributyl-(7-[1,3]dioxan-2-yl-benzofuran-5-yl)-stannane (1.43 g) and 4-bromo-3,5-dimethylisoxazole (0.51 g).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05935972uspto-grants-1999_08