반응 #1640

ord-1b2ca7107578479d93f1b4ae6d8fd313

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The resulting white solid (mp 87°-88° C.) was used in the next stage without further purification

실험 절차

The title compound was prepared from benzylhydroxymethylphosphinic acid, n-butyl ester and 4-chlorobenzenesulfonyl chloride according to the method described in Procedure 32. The resulting white solid (mp 87°-88° C.) was used in the next stage without further purification.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05726165uspto-grants-1998_03