반응 #1631

반응 방정식

cyclohexylphosphinic acid, n-butyl ester

paraformaldehyde

→

title compound

Cyclohexylhydroxymethylphosphinic acid, n-butyl ester

반응 조건

후처리

1. 1
   기타Purification by chromatography
2. 2
   세척eluting with dichloromethane containing 5% methanol
3. 3
   기타gave an oil

실험 절차

The title compound was prepared from cyclohexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

출처