반응 #1619
ord-a3c93df638364213adea34d2adfb06d5
반응 방정식
(R)-3-(3,4-dimethoxyphenyl)-2-propylamine
hydrogen bromide
→
title compound
(R)-3-(3,4-Dihydroxyphenyl)-2-propylamine hydrobromide
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도After cooling
- 2기타the solvent was evaporated
- 3기타the residue was dried
실험 절차
A solution of (R)-3-(3,4-dimethoxyphenyl)-2-propylamine hydrochloride1 (500 mg, 2.15 mMol) in hydrogen bromide (48%, 5 ml) was stirred at 100° C. under an argon atmosphere for 20 hours. After cooling, the solvent was evaporated and the residue was dried giving the title compound.