반응 #160960

ord-9cd77a866ae34b0c9f90ca13a7d7513f

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타to afford an off-white crystalline solid

실험 절차

The title compound was prepared in an analogous fashion to that described in Stage 9.3 using 5-bromo-6-chloro-nicotinic acid and 4-(perfluoroethoxy)aniline to afford an off-white crystalline solid. HPLC (Condition 4) tR=6.73 min, UPLC-MS (Condition 3) tR=1.30 min, m/z=443.1 [M−H]−.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08829195B2uspto-grants-2014_09