반응 #160960
ord-9cd77a866ae34b0c9f90ca13a7d7513f
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타to afford an off-white crystalline solid
실험 절차
The title compound was prepared in an analogous fashion to that described in Stage 9.3 using 5-bromo-6-chloro-nicotinic acid and 4-(perfluoroethoxy)aniline to afford an off-white crystalline solid. HPLC (Condition 4) tR=6.73 min, UPLC-MS (Condition 3) tR=1.30 min, m/z=443.1 [M−H]−.