반응 #160951

반응 방정식

5-bromo-6-chloro-nicotinic acid

4-pentafluoroethyl-aniline

→

title compound

5-Bromo-6-chloro-N-(4-(perfluoroethyl)phenyl)nicotinamide

반응 조건

후처리

1. 1
   기타to afford a white crystalline solid

실험 절차

The title compound was prepared in an analogous fashion to that described in Stage 11.2 using 5-bromo-6-chloro-nicotinic acid and 4-pentafluoroethyl-aniline to afford a white crystalline solid. HPLC (Condition 4) tR=6.61 min, UPLC-MS (Condition 3) tR=1.32 min, m/z=429 [M−H]−.

출처