반응 #1600740

반응 방정식

1-isopulegol

→

1-menthol

반응 조건

후처리

1. 1
   기타was carried out at 70° C. under a hydrogen
2. 2
   여과filtration and distillation of the reaction solution

실험 절차

By adding 0.45 g of Raney nickel to 283.8 g of the thus obtained 1-isopulegol, 10 hours of hydrogenation was carried out at 70° C. under a hydrogen pressure of 2.5 MPa. By carrying out filtration and distillation of the reaction solution, 273.5 g (1.75 mol, 71.24% e.e.) of 1-menthol was obtained.

출처