반응 #1596996

ord-128b3b4e09954149a920b362c22a9eb1

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타in Synthesis Example 1

실험 절차

By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 4-chlorobenzyl chloride (630 mg, 3.91 mmole), 480 mg (53% yield) of 5-(4-chlorobenzyl)aminosalicylic acid was obtained as a white solid.:mp 227-228° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08211877B2uspto-grants-2012_07