반응 #1596995

ord-84289a27ef1a4e41b17689cb80d0be1e

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타in Synthesis Example 1

실험 절차

By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (2.00 g, 13.0 mmole) and 4-nitrobenzyl bromide (3.38 g, 15.6 mmole), 2.90 g (79% yield) of 5-(4-nitrobenzyl)aminosalicylic acid was obtained as a pale yellow solid.:mp 211-212° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08211877B2uspto-grants-2012_07