반응 #1596978
ord-2dfc2ce301f24088acdd8e062b4dee75
반응 방정식
N-methylpiperazine
2-(2′-nitro-5′-fluorophenyl)benzothiazole
K2CO3
→
2-(2′-Nitro-5′-(N-methylpiperazinyl)phenyl)benzothiazole
반응 조건
온도
90°CELSIUS
상세 조건
See reaction.notes.procedure_details.
실험 절차
0.31 g (0.0030 mol) of N-methylpiperazine was added to the mixture of 0.41 g (0.015 mol) of 2-(2′-nitro-5′-fluorophenyl)benzothiazole and 0.32 g (0.0023 mol) of K2CO3 in 5 ml of dimethyl sulfoxide. The reaction was stirred magnetically and heated at 90° C., the progression thereof being verified by TLC.