반응 #159617

ord-9f50c0c70a1044b5ab00b3b845761f4a

반응 방정식

Cl.OC1CNC1
azetidin-3-ol hydrochloride
COC(=O)c1cc(F)cnc1Cl
methyl 2-chloro-5-fluoronicotinate
COC(=O)c1cc(F)cnc1N1CC(O)C1
title compound ( D70 )
COC(=O)c1cc(F)cnc1N1CC(O)C1
methyl 5-fluoro-2-(3-hydroxyazetidin-1-yl)nicotinate

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title compound (D70) (75 mg) was prepared according to the experimental procedure described in Description 62 starting from azetidin-3-ol hydrochloride (208 mg, 1.89 mmol) and methyl 2-chloro-5-fluoronicotinate (300 mg, 1.58 mmol, commercially available from Adesis#2-482).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08828987B2uspto-grants-2014_09