반응 #1594085

ord-e1d781dfe50d42bb9df9ad74b420ce7b

반응 방정식

CCOC(=O)c1c(NS(=O)(=O)c2ccccc2)sc2c1CCCC2
Intermediate 1
CCOC(=O)c1c(NS(=O)(=O)c2ccccc2)sc2c1CCCC2
ethyl 2-benzenesulphonylamino-4,5,6,7-tetrahydro-benzo[b]thiophene-3-carboxylate
CCOC(=O)c1cc(-c2ccccc2)sc1N
ethyl 2-amino-5-phenylthiophene-3-carboxylate
O=S(=O)(Cl)c1ccccc1
benzenesulphonyl chloride
→
CCOC(=O)c1cc(-c2ccccc2)sc1NS(=O)(=O)c1ccccc1
Ethyl 2-benzenesulphonylamino-5-phenylthiophene-3-carboxylate

반응물

CCOC(=O)c1c(NS(=O)(=O)c2ccccc2)sc2c1CCCC2
Intermediate 1
CCOC(=O)c1c(NS(=O)(=O)c2ccccc2)sc2c1CCCC2
ethyl 2-benzenesulphonylamino-4,5,6,7-tetrahydro-benzo[b]thiophene-3-carboxylate
CCOC(=O)c1cc(-c2ccccc2)sc1N
ethyl 2-amino-5-phenylthiophene-3-carboxylate
O=S(=O)(Cl)c1ccccc1
benzenesulphonyl chloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Prepared

실험 절차

Prepared by proceeding in a similar manner to Intermediate 1, starting from ethyl 2-amino-5-phenylthiophene-3-carboxylate and benzenesulphonyl chloride

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09221787B2uspto-grants-2015_12