반응 #159282

ord-3e84eb0ed57b475cbbdee34bf3c5aaeb

시약

없음

반응 조건

온도
100°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Excess butyric anhydride was then removed under reduced pressure
  2. 2
    기타to provide a solid residue that
  3. 3
    기타was recrystallized from ethanol

실험 절차

5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08828960B2uspto-grants-2014_09