반응 #159282
ord-3e84eb0ed57b475cbbdee34bf3c5aaeb
반응 조건
온도
100°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타Excess butyric anhydride was then removed under reduced pressure
- 2기타to provide a solid residue that
- 3기타was recrystallized from ethanol
실험 절차
5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.