반응 #158942

ord-9ffbde8b327a4cbd91a07fff2f05372a

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타rt=2.39 min.

실험 절차

2-[2-({[2-(4-Bromo-phenyl)-2-oxo-ethylcarbamoyl]-methyl}-tert-butoxycarbonyl-amino)-acetylamino]-3-methyl-butyric acid was prepared using method 801 substituting 2-[2-({[2-(4-bromo-phenyl)-2-oxo-ethylcarbamoyl]-methyl}-tert-butoxycarbonyl-amino)-acetylamino]-3-methyl-butyric acid methyl ester for 4-oxo-hexahydro-pyrrolo[1,2-a]pyrazine-2,6-dicarboxylic acid 6-ethyl ester 2-methyl ester. C22H30BrN3O7 calculated 527.1 observed [M+1]+ 528.1; rt=2.39 min.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08822430B2uspto-grants-2014_09