반응 #157904
ord-81dc4ea8c152498aaf44befe36b0dc78
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타is in the temperature range of about 85° C. to about 95° C
- 2기타to form a dark slurry
- 3기타resulted
- 4여과The product was filtered in a Büchner funnel
- 5세척the cake was washed with deionized water
- 6기타drying
실험 절차
200 g of disodium tetraborate was dissolved in 800 ml of hot deionized water. The water is in the temperature range of about 85° C. to about 95° C. 150 g of 45% titanium III sulfate was added to the above solution to form a dark slurry. 35% H2O2 was added drop-wise to the slurry until a homogenous yellow suspension resulted. The product was filtered in a Büchner funnel, and the cake was washed with deionized water. Solids were determined to be 19.8% by oven drying.