반응 #1578272

ord-e4305e6b5dfb41ec99bb8dae428f38fa

반응 방정식

CC(C)(Cc1ccccc1)C(=O)Nc1c(F)c(F)c(C(F)(F)F)c(F)c1F
CC(C)(Cc1ccccc1)C(=O
→
CC(CB1OC(C)(C)C(C)(C)O1)(Cc1ccccc1)C(=O)Nc1c(F)c(F)c(C(F)(F)F)c(F)c1F
CC(CB1OC(C)(C)C(C)(C
수율 77.0%

반응물

CC(C)(Cc1ccccc1)C(=O)Nc1c(F)c(F)c(C(F)(F)F)c(F)c1F
CC(C)(Cc1ccccc1)C(=O)Nc1c(F)c(
CAS: 1257521-29-1

시약

CC(=O)O.[Pd]
CC(=O)O.[Pd]
CAS: 3375-31-3
COc1cc(OC)c2ccccc2n1
COc1cc(OC)c2ccccc2n1
CAS: 40335-00-0
CC1(C)OB(B2OC(C)(C)C(C)(C)O2)OC1(C)C
CC1(C)OB(B2OC(C)(C)C(C)(C)O2)O
CAS: 73183-34-3
CC(=O)O
CC(=O)O
CAS: 64-19-7
O=C(O)O.[K]
O=C(O)O.[K]
CAS: 298-14-6
CC[N+](CC)(CC)CC.F[B-](F)(F)F
CC[N+](CC)(CC)CC.F[B-](F)(F)F
CAS: 429-06-1

용매

CC#N
CC#N
CAS: 75-05-8

반응 조건

온도
80°CELSIUS

출처

DOI: 10.1002/anie.201509996Borylation dataset from Roche