반응 #157635

반응 방정식

2-amino-4-fluorobenzenethiol

methyl 2-(bromomethyl)benzoate

K2CO3

→

title compound

수율 63.1%

methyl 2-(((2-amino-4-fluorophenyl)thio)methyl)benzoate

수율 63.1%

용매

DMF

반응 조건

실험 절차

Following General Procedure A, the title compound (1.8 g, 60%) was prepared from 2-amino-4-fluorobenzenethiol (1.4 g, 9.79 mmol) and methyl 2-(bromomethyl)benzoate (2.2 g, 9.79 mmol), K2CO3 (4.0 g, 29.4 mmol) in DMF (50 ml).

출처