반응 #157188
ord-a8838e4c9271477f88911011941c5767
반응 방정식
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
K2CO3 (2.45 g, 17.7 mmol), Dry DMF (5.4 mL), 1,5-Dihydroxy-naphthalene-2-carboxylic acid (0.539 g, 2.64 mmol), benzyl chloride (1.5 mL) Yield: 0.68 g of product (54%, 2 steps) Rf=0.38 (SiO2, 15% Hexanes/CH2Cl2). 1H NMR (400 MHz, CDCl3) δ 5.12 (s, 2H), δ 5.25 (s, 2H), δ 5.40 (s, 2H), δ 6.98 (d, J=7.3 Hz, 1H), δ 7.30-7.53 (m, 16H), δ 7.83 (d, J=8.7 Hz, 1H), δ 7.89 (d, J=8.7 Hz, 1H), δ 8.14 (d, J=8.7 Hz, 1H).