반응 #1563941

반응 방정식

KSCN

Benzyl 1-methylcyclopropane-1-sulfonate

→

Potassium 1-methylcyclopropane-1-sulfonate

용매

DME H2O

반응 조건

후처리

1. 1
   기타Reaction mixture
2. 2
   농축was concentrated under reduced pressure
3. 3
   세척the residue was washed with n-Pentane
4. 4
   기타dried

실험 절차

KSCN (2.48 g, 25.5 mmol) was added to a solution of Benzyl 1-methylcyclopropane-1-sulfonate (4.9 g, 25.5 mmol) in DME/H2O (1:1, 120 mL) and continued stirring at 100° C. for 16 h. Reaction mixture was concentrated under reduced pressure and the residue was washed with n-Pentane and dried to afford Potassium 1-methylcyclopropane-1-sulfonate (Int-26) which was used in the next step without further purification.

출처