반응 #1552054

반응 방정식

methyl-4-bromobenzoate

hydrazine monohydrate

→

white solid

수율 67.0%

4-bromobenzohydrazide

수율 67.0%

용매

ethanol

반응 조건

후처리

1. 1
   온도the mixture was heated
2. 2
   workup.STIRRINGstirred at 78° C. for 5 hours
3. 3
   기타A solid obtained
4. 4
   세척washed with water
5. 5
   여과collected by suction filtration

실험 절차

First, 3.0 g (13.9 mmol) of methyl-4-bromobenzoate was put in a 100-mL three-neck flask, 10 mL of ethanol was added therein, and the mixture was stirred. Thereafter, 4.0 mL of hydrazine monohydrate was added therein, and the mixture was heated and stirred at 78° C. for 5 hours. A solid obtained washed with water and collected by suction filtration; thus, 2.0 g of a white solid of objective 4-bromobenzohydrazide was obtained (yield: 67%).

출처