반응 #1552043
ord-5457b3292eac4bc197a3beacfcc105ba
반응 방정식
N-methoxy-acrylamide
chloroformic acid vinyl ester
→
title compound
N-Methoxy-N-propenoylcarbamic acid vinyl ester
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타Purification by column chromatography on silica gel (PE:EE=9:1)
실험 절차
The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.