반응 #1552022

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iodine monochloride

1-chloro-9-iodoperfluorononane

perfluorocyclopropane

1-chloro-11-iodoperfluoroundecane

→

1-chloro-3-iodoperfluoropropane

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후처리

1. 1
   기타can be obtained

실험 절차

As for a compound in which n is 9 or 11 in formula (22), 1-chloro-9-iodoperfluorononane (22-4) or 1-chloro-11-iodoperfluoroundecane (22-5) can be obtained by allowing iodine monochloride to react with commercially available perfluorocyclopropane (53) at a high temperature to obtain 1-chloro-3-iodoperfluoropropane (54), and then allowing 1-chloro-3-iodoperfluoropropane (54) to react with tetrafluoroethylene (51) under high temperature and pressurized conditions.

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