반응 #1543034

반응 방정식

N-(2-mercaptoethyl)glutaramic acid

ammonia

→

N-(2-Mercaptoethyl)glutaramide

반응 조건

후처리

1. 1
   기타After evaporation
2. 2
   기타to dryness and recrystallization from isopropanol 7 g of N-(2-mercaptoethyl)glutaramide
3. 3
   기타were obtained in the form of a white solid with a melting point of 127° C.

실험 절차

A solution of 9.1 g (44 mmol) of methyl ester of N-(2-mercaptoethyl)glutaramic acid obtained in Example 4a), in 100 cm3 of aqueous 20% solution of aqueous ammonia was stirred for 4 hours at ambient temperature under argon atmosphere. After evaporation to dryness and recrystallization from isopropanol 7 g of N-(2-mercaptoethyl)glutaramide were obtained in the form of a white solid with a melting point of 127° C.

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