반응 #1543032

ord-574d33b32a0247a1b1df185e92f30c92

반응 방정식

O=C(O)CCC(=O)NCCS
N-(2-mercaptoethyl)succinamic acid
NCCO
ethanolamine
O=C(CCC(=O)NCCS)NCCO
N-(2-mercaptoethyl)-N'-(2-hydroxyethyl)succinamide

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

A solution of 4.4 g (23 nmnol) of methyl ester of N-(2-mercaptoethyl)succinamic acid obtained in Example 1a) in 20 cm3 of methanol, and 1.68 g (27 mmol) of ethanolamine was stirred for 5 hours at 60° C. under argon atmosphere.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05843416uspto-grants-1998_12