반응 #1541934

반응 방정식

potassium

3-oxo-2-cyanopropanoic acid t-butyl ester

triphenylsulfonium chloride

water

→

3-oxo-2-cyanopropanoic acid t-butyl ester triphenylsulfonium salt

수율 79.0%

반응 조건

실험 절차

COMP CD-8 was prepared similar to COMP CD-7 at 79% yield from potassium salt of 3-oxo-2-cyanopropanoic acid t-butyl ester (2.07 g, 10 mmol) and 50% solution of triphenylsulfonium chloride in water (5.96 g, 10 mmol) as a yellow color, light weight (fluffy) crystalline material.

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