반응 #1535778

ord-c515cc8a7e464c828fc55376f0dc42ff

반응 방정식

CC(C)c1cc(O)cc(O)c1
5-Isopropyl resorcinol
CC(C)N1CCC(=O)CC1
N-isopropyl-4-piperidone
Cl
HCl
→
CC(C)c1cc(O)c(C2=CCN(C(C)C)CC2)c(O)c1.Cl
product
수율 50.0%
CC(C)c1cc(O)c(C2=CCN(C(C)C)CC2)c(O)c1.Cl
2-(N-Isopropyl-1,2,3,6-tetrahydro-4-pyridyl)-5-isopropyl resorcinol hydrochloride
수율 50.0%

반응물

CC(C)c1cc(O)cc(O)c1
5-Isopropyl resorcinol
CC(C)N1CCC(=O)CC1
N-isopropyl-4-piperidone
Cl
HCl

시약

없음

용매

CC(=O)O
acetic acid

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

5-Isopropyl resorcinol (5.40 g), N-isopropyl-4-piperidone (5.00 g) and 12 ml acetic acid was treated with HCl as described in Example I to give 5.48 g product (50% yield); m.p. 247°-248°.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04180669uspto-grants-1979_12