반응 #1534736

반응 방정식

ethylene diacrylate

methyl methacrylate

Emulphor ON-870

potassium persulfate

sodium bisulfite

N,N-diethylaminoethyl methacrylate

→

N,N-diethylaminoethyl acrylate

methyl methacrylate

용매

water

반응 조건

후처리

1. 1
   workup.ADDITIONmixed with 1,000 g

실험 절차

50 Grams of N,N-diethylaminoethyl methacrylate, 50 g. of methyl methacrylate, 1 g. of Dupanol ME, 1 g. of Emulphor ON-870, 6 g. of ethylene diacrylate, 1 g. of potassium persulfate, and 0.5 g. of sodium bisulfite are dissolved or mixed with 1,000 g. of water. This mixture is tumbled in a water bath at 60° C. for 24 hr. to obtain a crosslinked copolymer of methyl methacrylate and N,N-diethylaminoethyl acrylate. The crosslinked polymer is separated from the aqueous dispersion by the method described in Example 4.

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