반응 #1521115

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1-bromo-3,4-dimethoxybenzene

1-bromo-4,5-dimethoxy-2-nitrobenzene

7-benzyloxy-3-bromo-1,2-dihydronaphthalene

→

7-benzyloxy-3-(4,5-dimethoxy-2-nitrophenyl)-1,2-dihydronaphthalene

수율 21.8%

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후처리

1. 1
   기타were used according to an analogous synthetic method to Preparation Example 107

실험 절차

Synthesized from 1-bromo-3,4-dimethoxybenzene according to an analogous synthetic method to Preparation Example 108, 1-bromo-4,5-dimethoxy-2-nitrobenzene (7.5 g) and 7-benzyloxy-3-bromo-1,2-dihydronaphthalene (4.5 g) were used according to an analogous synthetic method to Preparation Example 107 to provide 7-benzyloxy-3-(4,5-dimethoxy-2-nitrophenyl)-1,2-dihydronaphthalene (1.3 g). The total amount of this compound was used according to an analogous synthetic method to Example 30 to provide the title compound (822 mg).

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