반응 #1519114

ord-5d275247c288445f9962bcfcedeb8294

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타purified by preparative reverse-phase (C18) HPLC

실험 절차

3-aminocarbonylpropionate A-6 (0.1 mmol) is treated with dioxane (1 mL) and hydroxylamine (50% in water, 2 mL) for 1-3 days, and then purified by preparative reverse-phase (C18) HPLC to afford the desired N-hydroxy-3-aminocarbonylpropionamide (A-7).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07612059B2uspto-grants-2009_11