반응 #1519091

ord-35da2e9cf1e04c2bae28be44c28b71c9

반응 방정식

OCCOCCOCCO
triethylene glycol
COCCOCCOCCOCCOCCOCCOCCOS(C)(=O)=O
compound 31
COCCOCCOCCOCCOCCOCCOCCOS(C)(=O)=O
20-methoxy-1-(methylsulfonyl)oxy-3,6,9,12,15,18-hexaoxaeicosane
CO
methanol
COCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO
compound 32
COCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO
Decaethylene glycol monomethyl ether

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Monodispersed compound 32 was prepared from compound 31 and monodispersed triethylene glycol using the procedure described above in Example 17. Oil; Rf 0.41 (methanol:chloroform=6:10); MS m/z calc'd for C21H44O11 472.29 (M++1), found 472.29.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07611864B2uspto-grants-2009_11