반응 #1518

반응 방정식

4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester

hydrogen

→

4-(6-decyloxy-2-naphthoyloxy)benzoic acid

수율 97.5%

용매

THF

반응 조건

후처리

1. 1
   여과filtered

실험 절차

To 37.6 g (0.07 mol) of the 4-(6-decyloxy-2-naphthoyloxy)benzoic acid benzyl ester obtained in the first stage was added 3.76 g of 5% palladium/carbon, and further added 188 g of THF. Then, hydrogen gas was blown into the mixture. The resultant mixture was stirred overnight and filtered to obtain 30.6 g of 4-(6-decyloxy-2-naphthoyloxy)benzoic acid.

출처