반응 #1490859

반응 방정식

2-mercapto-ethanol

DIEA

3-bromo-dihydro-furan-2-one

→

3-(2-Hydroxy-ethylsulfanyl)-dihydro-furan-2-one

용매

THF

반응 조건

후처리

1. 1
   여과The precipitate was filtered
2. 2
   기타the solvent was removed under reduced pressure

실험 절차

To a solution of 2-mercapto-ethanol (2560 μmol) in THF (4 ml) were added DIEA (1.1 eq) and 3-bromo-dihydro-furan-2-one (1 eq). The reaction mixture was stirred at RT for 4 hours. The precipitate was filtered and the solvent was removed under reduced pressure.

출처