반응 #1478592

반응 방정식

4-carboxybenzaldehyde

trimethylsilyl chloride

→

4-methoxycarbonylbenzaldehyde

용매

MeOH

반응 조건

후처리

1. 1
   기타After evaporation

실험 절차

The 4-carboxybenzaldehyde is of commercial origin. It is dissolved (3 g; 20 mmol) in a trimethylsilyl chloride solution (10 g; 92 mmol) in 100 ml of MeOH. The mixture is kept stirred for 40 h at room temperature. After evaporation, a white solid corresponding to 4-methoxycarbonylbenzaldehyde 24 is isolated, characterized by NMR and used as it is for the next reaction.

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