반응 #1470442

ord-7776a422853646679ef31d1498c4d055

반응 방정식

OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose
OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
TREHAOSE
[Cl-].[Cl-].[Mg+2]
magnesium chloride
O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate

용매

반응 조건

온도
118°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    세척Soybeans were washed with water
  2. 2
    기타to obtain
  3. 3
    기타had been prepared
  4. 4
    workup.WAITcontinued boiling for about 10 min
  5. 5
    농축concentrate the soybeans until the solution
  6. 6
    workup.WAITventilated for five hours with air
  7. 7
    온도heated to 35° C.

실험 절차

Soybeans were washed with water and soaked in 4-time volumes of water for six hours, and then boiled and placed on a sieve to obtain boiled beans. The beans were soaked in a 60% aqueous trehalose solution containing 0.1% magnesium chloride at 70° C. for three hours, and taken out of the solution. Five parts by weight of the resulting beans were soaked in a solution, which had been prepared by dissolving in 35 parts by weight of water about 80 parts by weight of “TREHAOSE®”, a high-purity crystalline trehalose hydrate commercialized by Hayashibara Shoji, Inc., Okayama, Japan, and had been boiling at about 115° C. under normal atmospheric pressure, and continued boiling for about 10 min to dehydrate and concentrate the soybeans until the solution was heated to about 118° C. Thereafter, the fried beans were placed on a plain sieve, sprayed with a small amount of a high-purity trehalose hydrate, and ventilated for five hours with air heated to 35° C. to obtain a non-fried fresh tea leaf coated with crystalline trehalose dihydrate by crystallizing the saccharide thereon.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06254912B1uspto-grants-2001_07