반응 #1470424

반응 방정식

1-oxyl-2,2,6,6-tetramethyl-4-hydroxypiperidine

epichlorohydrin

→

title compound

1-Oxyl-2,2,6,6-tetramethyl-4-glycidyloxypiperidine

용매

sodium hydroxide

toluene

반응 조건

후처리

1. 1
   기타is reacted together
2. 2
   건조The organic phase is dried over anhydrous magnesium sulfate
3. 3
   농축concentrated

실험 절차

A vigorously stirred two phase solution of 1-oxyl-2,2,6,6-tetramethyl-4-hydroxypiperidine, epichlorohydrin, tetrabutylammonium bromide in 50% aqueous sodium hydroxide and toluene is reacted together. The organic phase is dried over anhydrous magnesium sulfate and concentrated to yield the title compound as a low melting red solid after column chromatography.

출처