반응 #1463483

반응 방정식

cyclohexane

4-(4-propylphenyl)phenylcyclohexane

toluene

formic acid

→

3-(4-(4-(4-propylphenyl)phenyl)cyclohexyl)propanal

반응 조건

후처리

1. 1
   온도heating the mixture
2. 2
   온도under reflux for 5 hours
3. 3
   세척washing the reaction mixture with water after completion of the stirring
4. 4
   건조drying over anhydrous magnesium sulfate
5. 5
   농축concentrating under reduced pressure
6. 6
   기타isolating the resulting yellow oil

실험 절차

This cyclohexane derivative (11.8 g, 30 mmols) was dissolved in toluene (100 ml), followed by adding formic acid (5 ml), heating the mixture under reflux for 5 hours, washing the reaction mixture with water after completion of the stirring, drying over anhydrous magnesium sulfate, concentrating under reduced pressure and isolating the resulting yellow oil to obtain 3-(4-(4-(4-propylphenyl)phenyl)cyclohexyl)propanal. This product is used in the subsequent reaction with any purification.

출처