반응 #1443781
ord-fd3b100d1e6a477587f1c31f9a45de8e
반응 조건
온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타adjusted to a temperature of 20° C.
- 2온도After cooling
- 3기타the liquid sample (1.9 g) was recovered
실험 절차
CF3(CF2)9OCF(CF3)CF2OCOCF(CF3)OCF2CF2CF3 (2.0 g) obtained in Example 23 was charged into a flask together with a NaF powder (0.05 g) and heated at 150° C. for 24 hours in an oil bath with vigorous stirring. At an upper part of the flask, a reflux condenser adjusted to a temperature of 20° C., was installed. After cooling, the liquid sample (1.9 g) was recovered. By GC-MS, it was confirmed that CF3CF(OCF2CF2CF3)COF and the above-identified compound were the main products. The yield was 63.8%.