반응 #1435718

반응 방정식

potassium hydride

(2-trimethylsiloxy-ethyl)-cyclopentadiene

→

potassium (2-trimethylsiloxy-ethyl)-cyclopentadienide

수율 81.0%

용매

tetrahydrofurane

tetrahydrofurane

반응 조건

후처리

1. 1
   workup.ADDITIONis added
2. 2
   온도The reaction is maintained
3. 3
   기타leaving an oily solid which
4. 4
   세척is washed with hexane in order
5. 5
   기타to obtain a brown solid

실험 절차

To a suspension of 0.5 g (12.4 mmol) of potassium hydride in tetrahydrofurane, 2.25 g (12.4 mmol) of (2-trimethylsiloxy-ethyl)-cyclopentadiene in tetrahydrofurane is added. The reaction is maintained under stirring for 2 hours and then the volatile compounds are eliminated, leaving an oily solid which is washed with hexane in order to obtain a brown solid. (2.2 g Yield: 81%)

출처