반응 #1428

반응 방정식

α-methyl cinnamic acid

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title product

α-Methyl-hydrocinnamic acid

용매

methanol

methanol

반응 조건

후처리

1. 1
   여과filtered through a Celite pad in a millipore unit
2. 2
   세척washing the pad well with methanol (2×100 ml.)
3. 3
   기타The clear filtrate was evaporated to dryness
4. 4
   기타to give 10.225 g

실험 절차

A solution of α-methyl cinnamic acid (10.0 g., 61.7 mmol.) in dry methanol (250 ml.) was treated with 10% palladium on carbon and hydrogenated (balloon used) at room temperature for 16 hours. The reaction mixture was diluted with methanol (250 ml.), filtered through a Celite pad in a millipore unit, washing the pad well with methanol (2×100 ml.). The clear filtrate was evaporated to dryness to give 10.225 g. of title product as a thick syrup.

출처