반응 #1400

반응 방정식

4,4'-difluorodiphenylmethane

sulfuric acid

→

4,4'-difluorobenzophenone

수율 54.0%

용매

water

반응 조건

후처리

1. 1
   workup.ADDITIONare first mixed
2. 2
   workup.ADDITIONis added

실험 절차

The procedure of Example 2 is used except that the 4,4'-difluorodiphenylmethane, water, and sulfuric acid are first mixed, then heated before the MnO2 is added. The yield is 54% 4,4'-difluorobenzophenone that is 95% pure.

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