반응 #1381627
ord-ddecc81dca0e455d8001062829ecfc78
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타crystallized three times from several volumes of acetone at 1° C.
실험 절차
Erythritol and a five-fold molar excess of methyl oleate are heated at 180° C. under vacuum, with agitation, in the presence of sodium methoxide catalyst over two reaction periods of several hours each. The reaction product (predominately erytiritol tetraoleate) is refined in petroleum ether and crystallized three times from several volumes of acetone at 1° C.