반응 #1370437

ord-4e0b2256045d47b990da82be858649a7

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

In this process, the reaction product of phenyldichlorophosphine and p-cyanophenyl-diazonium-tetrafluoroborate has to be subjected to a reduction with aluminum in order to obtain the p-cyanophenyl-phenylchlorophosphine. The yield is 47 % of the theoretical yield. This process can be carried out only with difficulty on a large scale, and the formation of large amounts of fluorine containing waste secondary products creates the problem of the pollution-free destruction thereof.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US03974243uspto-grants-1976_08