반응 #1369

반응 방정식

2-methyl-3,4,6-trifluorobenzoic acid

chloride

→

2-methyl-3,4,6-trifluorobenzoyl chloride

반응 조건

후처리

1. 1
   온도the mixture is refluxed for 1 hour
2. 2
   농축After concentrating

실험 절차

To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.

출처