반응 #1365706

ord-8df9a23df07745eab43ba41bd6dfb9e9

반응 방정식

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid
COc1ccc(C=O)cc1.O=S(=O)(O)O
Anisaldehyde sulfuric acid

용매

반응 조건

온도
100°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06444233B1uspto-grants-2002_09