반응 #1350565

반응 방정식

N-butyl-N-cyclooctylpyrrolidinium iodide salt

hydroxide

→

N-butyl-N-cyclooctylpyrrolidinium hydroxide

용매

water

반응 조건

후처리

1. 1
   workup.ADDITIONof Ion Exchange Resin OH (BIO RAD® AG1-X8) was added
2. 2
   여과The mixture was filtered
3. 3
   세척the solids were rinsed with an additional 250 ml
4. 4
   여과The original mixture was filtered

실험 절차

N-butyl-N-cyclooctylpyrrolidinium iodide salt (95 gms., 0.26 mole) was dissolved in 300 ml. water in a 1000 ml. plastic bottle. To the solution, 300 gms. of Ion Exchange Resin OH (BIO RAD® AG1-X8) was added and the mixture was stirred at room temperature overnight. The mixture was filtered and the solids were rinsed with an additional 250 ml. of water. The original mixture was filtered and the rinse were combined and a small amount was titrated with 0.1N HCl to indicate the presence of 0.24 mol hydroxide (0.24 mol N-butyl-N-cyclooctylpyrrolidinium hydroxide) in the solution.

출처