반응 #1338161

반응 방정식

2-Cyanoethyldichlorophosphite

4-(trimethylsilyl)pyrrolidine

→

oil

수율 103.5%

Chloro(2-Cyanoethyoxy)pyrrolidinophosphine

수율 103.5%

용매

CH2Cl2

반응 조건

후처리

1. 1
   기타The solvent was removed under the reduced pressure

실험 절차

To a solution of 2-Cyanoethyldichlorophosphite (2.0 g, 11.6 mmol, 1.5 mL) in CH2Cl2 (30 mL) was added dropwise 4-(trimethylsilyl)pyrrolidine (2.0 mL, 1.7 g, 11.6 mmol) at 0° C. The resulting mixture was stirred overnight at room temperature. The solvent was removed under the reduced pressure to give a colorless oil (2.48 g, 88%) as a product.

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