반응 #1338160

반응 방정식

2-Cyanoethyldichlorophosphite

4-(trimethylsilyl)morpholine

→

oil

수율 99.3%

Chloro(2-Cyanoethoxy)morpholinophosphine

수율 99.3%

용매

CH2Cl2

반응 조건

후처리

1. 1
   기타The solvent was removed under reduced pressure

실험 절차

To a solution of 2-Cyanoethyldichlorophosphite (3.0 g, 17.5 mmol, 2.2 mL) in CH2Cl2 (45 mL) was added dropwise 4-(trimethylsilyl)morpholine (3.1 mL, 2.8 g, 17.5 mmol) at 0° C. The resulting mixture was stirred for 2 h at room temperature. The solvent was removed under reduced pressure to give a pale yellow oil (3.87 g, 86%) as a product.

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