반응 #1286459

반응 방정식

ethyl perfluorobutyrate

dimethylamine

→

N,N-Dimethyl Perfluorobutyramide

반응 조건

후처리

1. 1
   기타A 3-necked flask, equipped with magnetic stirrer
2. 2
   온도reflux condenser and gas inlet tube
3. 3
   기타in the range of 60°-70° C.
4. 4
   온도increase of the flask

실험 절차

A 3-necked flask, equipped with magnetic stirrer, reflux condenser and gas inlet tube, was charged with 121 g (0.5 mole) of ethyl perfluorobutyrate. The contents of the flask were heated to 60° C. and a slow stream of dimethylamine was passed in. The reaction is exothermic and the gas flow rate was adjusted to keep the temperature in the range of 60°-70° C. without external heat. Gas flow was continued until the weight increase of the flask showed absorption of 22.5 g (0.5 mole) of the amine.

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